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I was so familiar with him that I recognized his voice I pick up the phone.

A. while B. after C. in case D. the instant

D

【解析】

試題分析：考查連詞辨析。A. while 當......的時候；B. after 在......之后；C. in case以防萬一； D. the instant一......就；“我對他如此熟悉以至于我一接起電話就認出了他的聲音”；故選D.

考點：考查連詞辨析。

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